DISTILLATION.

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The volatile oil obtained from many aromatic plants by steam distillation is often their most valuable product. The equipment necessary for distilling volatile oils consists essentially of a steam boiler, a retort, and a condenser. A constant supply of cold water must also be available. A common type of retort consists of a circular wooden vat, about 6 feet in diameter and 8 to 10 feet deep (fig. 4), fitted with a removable cover, which can be made steam tight. Metal retorts made of boiler iron three-sixteenths of an inch thick and jacketed with wood to prevent the radiation of heat are also used. A pipe leads from the steam boiler to the bottom of the retort and another from the top of the retort to the condenser, one form of which consists of a coil of tin-lined or galvanized-iron pipe inclosed in a jacket through which cold water is kept flowing when the still is in operation.

Fig. 4.—A still used in the production of wormwood oil.

When the retort is filled with aromatic plants and steam is admitted through the pipe from the boiler, the volatile oil is extracted in the form of a vapor, which is carried over with the steam to the condenser, where both are condensed to liquid form. The oil and water together flow from the condenser into the receiver, one type of which is constructed like an ordinary milk can and is fitted with a siphon leading from the bottom, through which the water is drawn off to prevent the receiver from overflowing.

Many volatile oils will float on the water and may be drawn off from the top of the receiver at will. Other oils, such as sassafras and wintergreen, are heavier than water, and should be collected in a receiver provided at the bottom with an outlet tap through which the oil may be drawn off.

The cost of setting up a still will depend upon what facilities are already at hand and upon the size and efficiency of the apparatus installed. It may easily range from a small sum to several thousand dollars.


                                                                                                                                                                                                                                                                                                           

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